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obrazek nr 1

Publikacje

PUBLIKACJE [2010 – 2020]

91. Kaczor-Keller Katarzyna B., Pawlik Anna, Ścianowski Jacek, Pacuła Agata, Obieziurska Magdalena, Marcheggiani Fabio, Cirilli Ilenia, Tiano Luca, Antosiewicz Jędrzej, In vitro anti-prostate cancer activity of two ebselen analogues, Pharmaceuticals, 2020, 13 no. 3, 1-16

90. Obieziurska Magdalena, Pacuła Agata J., Laskowska Anna, Długosz-Pokorska Angelika, Janecka Anna, Ścianowski Jacek, Seleninic acid potassium salts as water-soluble biocatalysts with enhanced bioavailability, Materials, 2020, 13 no.3, 1-12

89. Rabiej-Kozioł Dobrochna, Krzemiński Marek P., Szydłowska-Czerniak Aleksandra, Synthesis of steryl hydroxycinnamates to enhance antioxidant activity of rapeseed oil and emulsions, Materials, 2020, 13 no. 20, 1-13

88. Mruk Julianna, Pazderski Leszek, Ścianowski Jacek, Wojtczak Andrzej, Structural and NMR spectroscopic studies of 2-phenylsulfanylpyridine and its analogues or derivatives, and their Au(III) chloride complexes, Inorg. Chim. Acta, 2020, 500, 1-12

87. Kmieciak A., Krzemiński M., Synthesis of 2-amino-apopinan-3-ol and applications of its derivatives in asymmetric reduction of ketones, Proceedings, 2019, 41 no. 1, 1-10

86. Dziuk B., Ośmiałowski B., Zarychta B., Ejsmont E., Chęcińska L., Symmetric Fluoroborate and its Boron Modification: Crystal and Electronic Structures, Crystals, 2019, 9, 662-677

85. Ośmiałowski Borys, Petrusevich Elizaveta F., Antoniak Magda A., Grela Izabela, Bin Jassar Mohammed A., Nyk Marcin, Luis Josep M., Jędrzejewska Beata, Zaleśny Robert, Jacquemin Denis, Controlling two-photon action cross section by changing a single heteroatom position influorescent dyes, J. Phys. Chem. Lett., 2020, 11 no. 15, 5920-5925.

84. Moshkina Tatyana N., Nosova Emiliya V., Kopotilova Alexandra E., Lipunova Galina N., Valova Marina S., Sadieva Leila K., Kopchuk Dmitry S., Slepukhin Pavel A., Zaleśny Robert, Ośmiałowski Borys, Charushin Valery N., Synthesis and photophysical studies of novel V-shaped 2,3-bis5-aryl-2-thienyl (dibenzo[f,h])quinoxalines, Asian J. Org. Chem., 2020, 9 no.4, 673-681

83. Obieziurska Magdalena, Pacuła Agata, Laskowska Anna, Długosz-Pokorska Angelika, Krzemiński Marek, Janecka Anna, Ścianowski Jacek, N-terpenyl benzisoselenazolones : evaluation of the particular structure-bioactivity relationship, Proceedings (MDPI), 2019, 41 no. 1, S. 1-5

82. Bożejewicz D., Witt K., Kaczorowska M., Ośmiałowski B., The Copper(II) Ions Solvent Extraction with a New Compound: 2,6-Bis(4-Methoxybenzoyl)-Diaminopyridine, Processes, 2019, 7, 954-964

81. Obieziurska, M.; Pacuła, A. J.; Długosz-Pokorska, A.; Krzemiński, M.; Janecka, A.; Ścianowski, J., Bioselectivity Induced by Chirality of New Terpenyl Organoselenium Compounds, Materials, 2019, 12, 3579-3591

80. Kwiatkowski, A., Kolehmainen E., Ośmiałowski B., Conformational and Tautomeric Control by Supramolecular Approach in Ureido-N-iso-propyl,N’-4-(3-pyridin-2-one)pyrimidine, Molecules 2019, 24, 2491

79. Zaleśny R., Szczotka N., Grabarz A., Ośmiałowski B., Jacquemin D., Design of two‐photon‐excited fluorescent dyes containing fluoroborylene groups, ChemPhotoChem, 2019, 3, 719-726

78. Grabarz A., Skotnicka A., Jedrzejewska B., Murugan N. Arul, Patalas F., Bartkowiak W., Jacquemin D., Ośmiałowski B., The Impact of the Heteroatom in Five-Membered Ring on the Photophysical Properties of Difluoroborates, Dyes Pigments, 2019, 170, 107481

77. Tarahhomi A., van der Lee A., Ośmiałowski B., A detailed theoretical and experimental study on the N-H, P=O and C=O stretching frequencies in two new phosphoric triamides and a statistical comparison with analogous structures, Polyhedron, 2019, 158, 215-224

76. Obieziurska, M.; Pacuła, A. J.; Juhas, U.; Antosiewicz, J.; Ścianowski, J. The influence of O/S exchange on the biocatalytical activity of benzisoselenazol-3(2H)-ones, Catalysts, 2018, 8, 493-507.

75. Pacuła, A. J.; Obieziurska, M.; Ścianowski, J.; Kaczor, K.; Antosiewicz, J. Water-dependent synthesis of biologically active diaryl diselenides, 2018, 19, 144-155.

74. Ośmiałowski B., Conformational equilibrium and substituent effects in hydrogen bonded complexes, Curr. Org. Chem., 2018, 22, 2182-2199

73. Jędrzejewska B., Skotnicka A., Laurent A., Pietrzak M., Jacquemin D., Ośmiałowski B., The Influence of the Nature of the Amino Group in Highly Fluorescent Difluoroborates Exhibiting Intramolecular Charge Transfer, J.Org. Chem., 2018, 83, 7779-7788

72. Kwiatkowski A., Jędrzejewska B., Józefowicz M., Grela I., Ośmiałowski B., The trans/cis photoisomerization in hydrogen bonded complexes with stability controlled by substituent effect: 3-(6-aminopyridin-3-yl)acrylate case study, RSC Adv., 2018, 8, 23698-23710

71. Jędrzejewska B., Grabarz A., Bartkowiak W., Ośmiałowski B., Spectral and physicochemical properties of difluoroboranyls containing N,N-dimethylamino group studied by solvatochromic methods Spectrochim. Acta A, 2018, 199, 86-95

70. Kaczorowska, M. A., Ośmiałowski, B., Collision Induced Dissociation of N-(Pyridin-2-yl)-Substituted Benzo(Thio)amides and N-(Isoquinolin-1-yl)Furan(Thiophene)-2-Carboxamides and their Difluoroboranyl Derivatives. Int. J. Mass Spectrom. 2018, 428, 35-42

69. Jędrzejewska, B.; Ośmiałowski, B., Difluoroboranyl Derivatives as Efficient Panchromatic Photoinitiators in Radical Polymerization Reactions. Polym. Bull. 2018, 75, 3267–3281

68. Pacuła, A. J.; Kaczor, K. B.; Wojtowicz, A.; Antosiewicz, J.; Janecka, A.; Długosz, A.; Janecki, T.; Ścianowski, New glutathione peroxidase mimetics—Insights into antioxidant and cytotoxic activity, J. Bioorg. Med. Chem. 2017, 25, 126-131

67. Ścianowski, J.; Szumera, J.; Pacuła, A. J.; Rafiński, Z., Reactivity of dipinanyl diselenides functionalized at the C-10-position with -CH2O(Se)Ph, -OH and -OCPh3 substituents, Arkivoc, 2017, 272-284

66. Krzemiński M., Szydłowska-Czerniak A., Rabiej D., (2E)-3-(4-hydroksy-3,5-dimetoksyfenylo)prop-2-enian oktylu i sposób jego otrzymywania, Biul. Urzędu Patentowego Wynalaz. Wzory Użytkowe, nr 26, 2017, S. 23, Zgłoszenie patentowe: 417498

65. Krzemiński M., Preparation of (1R, 2R, 3R, 5S)-(-)- isopinocampheol through a hydroboration-oxidation reaction, Comprehensive organic chemistry experiments for the laboratory classroom, Cambridge : Royal Society of Chemistry, 2017, 252-256 + electronic suppl. material S. 1-12

64. Krzemiński M., Preparation of isoborneol through the Wagner-Meerwein rearrangement reaction of (1R)-(+)-camphene, Comprehensive organic chemistry experiments for the laboratory classroom, Cambridge : Royal Society of Chemistry, 2017, 826-829 + electronic suppl. material s. 1-13

63. Krzemiński M., Asymmetric reduction of acetophenone with borane catalyzed by B-methoxy-oxazaborolidine, Comprehensive organic chemistry experiments for the laboratory classroom, Cambridge : Royal Society of Chemistry, 2017, 803-806 + electronic suppl. material s. 1-9

62. Kmieciak A., Krzemiński M., Chiral terpene auxiliaries IV : new monoterpene PHOX ligands and their application in the catalytic asymmetric transfer hydrogenation of ketones, Tetrahedron Asymm., 2017, 28, 467-472

61. Tafelska-Kaczmarek A., Krzemiński M., Ćwiklińska M., Asymmetric synthesis of benzofuryl β-amino alcohols by the transfer hydrogenation of α-functionalized ketones, Tetrahedron, 2017, 73, 3883-3897


60. Ścianowski, J.; Pacuła, A.; Zielińska-Błajet, M.; Wojtczak, A., New diphenyl diselenides o-substituted by an O(S,Se)-caranyl skeleton – synthesis and application in asymmetric reactions, New J. Chem.,2016, 40, 6697-6705

59. Ścianowski, J.; Szumera, J.; Kleman, P.; Pacuła, A. J., Synthesis and reaction of terpenyl diselenides functionalized with phenyl and naphthyl groups, Tetrahedron Asymm., 2016, 27, 238-245

58. Ścianowski, J.; Banach, A.; Pacuła, A. J., Terpenyl tellurides : synthesis and application in asymmetric epoxidation, Phosphorus Sulfur Silicon,2016, 191, 263-267

57. Pacuła, A. J.; Ścianowski, J., Terpenes as green starting materials for new organoselenium and organotellerium compounds, Curr. Green Chem., 2016, 3, 36-50

56. Rafiński, Z., Novel (-)-β-pinene-derived triazolium salts : synthesis and application in the asymmetric Stetter reaction, ChemCatChem, 2016, 8, 2599-2603

55. Rafiński, Z., Enantioselective benzoin condensation catalyzed by spirocyclic terpene-based N -heterocyclic carbens, Tetrahedron, 2016, 72, 1860-1867

54. Jastrzębska, A.; Piasta, A.; Kowalska, S.; Krzemiński, M.; Szłyk, E., A new derivatization reagent for determination of biogenic amines in wines, Journal of Food Composition and Analysis 2016, 48, 111-119

53. Bosiak, M. J., A convenient synthesis of 2-arylbenzo[b]furans from aryl halides and 2-halophenols by catalytic one-pot cascade method, ACS Catal. 2016, 6, 2429-2434

52. Bosiak, M. J.; Trzaska, P.; .; Kędziera, D. Adams, J., Synthesis and photoluminescence properties of star-shaped 2,3,6,7-tetrasubstituted benzo[1,2-b:4,5-b’]difurans, Dyes & Pigments, 2016, 129, 199-208

51. Banach, A.; Ścianowski, J.; Uzarewicz, M., Wojtczak, A., Terpenyl selenides : synthesis and application in asymmetric epoxidation, Eur. J. Org. Chem., 2015, 16, 3477-3485

50. Skowronek, P.; Ścianowski, J.; Pacuła, A.J.; Gawroński, J., Chirality transfer through sulfur or selenium to chiral propellers, RSC Advances, 2015, 5, 69441-69444

49. Ścianowski, J.; Pacuła, A.J.; Wojtczak, A., New and efficient methodology for the synthesis of chiral mono- and ditellurides, Tetrahedron: Asymmetry, 2015, 26, 400-403

48. Pacuła, A.J., Mangiavacchi, F.; Sancineto, L.; Lenardão, E. J.; Ścianowski, J., Santi, C., An update on “Selenium containing compounds from poison to drug candidates : a review on the GPx-like activity”, Curr. Chem. Biol., 2015, 9, 97-112

47. Ćwiklińska, M.; Krzemiński, M. P.; Tafelska-Kaczmarek, A., Chiral terpene auxiliaries III : spiroborate esters from (1R,2S,3R,5R )-3-amino-apopinan-2-ol as highly effective catalysts for asymmetric reduction of ketones with borane, Tetrahedron: Asymmetry 2015, 26, 1453-1458

46. Kujawa, J.; Guillen-Burrieza, E.; Arafat, H.; Kurzawa, M.; Wolan, A.; Kujawski, W. Food and Bioprocess Technology, 2015, 8, 2146–2158

45. Rafiński,Z.; Kozakiewicz, A., Enantioselective synthesis of chromanones bearing quaternary substituted stereocenters catalyzed by (1R)-camphor-derived N-heterocyclic carbenes, J. Org. Chem. 2015, 80, 7468-7476

44. Włodarczyk, J.; Wolan, A.; Rakowiecki, M.; Bosiak, M. J.; Budny, M., Synthesis of an all-cis intermediate of ticagrelor, Tetrahedron Lett. 2015, 56, 6093-6096

43. Bosiak, M. J.; Rakowiecki, M.; Wolan, A.; Szlachta, J.; Stanek, E.; Cycoń, D.; Skupień, K. Dyes and Pigments, 2015, 121, 79-87

42. Midura, W. H.; Ścianowski, J.; Banach, A.; Zając, A., Asymmetric synthesis of cyclopropyl phosphonates using chiral terpenyl sulfonium and selenonium ylides, Tetrahedron Asymm., 2014, 25, 1488-1493

41. Pacuła, A.; Ścianowski, J.; Aleksandrzak, K., Highly efficient synthesis and antioxidant capacity of N-substituted benzisoselenazol-3(2H)-ones, RSC Advances, 2014, 4, 48959-48962

40. Banach, A.; Ścianowski, J.; Ozimek, P., The use of sulfides derived from carane, p-menthane, pinane, and bornane in the synthesis of optically active epoxides, Phosphorus Sulfur Silicon., 2014, 189, 274-284

39. Ścianowski, J.; Rafiński, Z., Electrophilic selenium reagents : addition reactions to double bonds and selenocyclizations, Organoselenium chemistry : between synthesis and biochemistry / ed.: Santi. C./ Perugia : Bentham Science Publishers, 2014, 8-60

38. Rafiński, Z.; Kozakiewicz, A.; Rafińska, K., Highly efficient synthesis of spirocyclic (1R )-camphor-derived triazolium salts : application in the catalytic asymmetric benzoin condensation, Tetrahedron, 2014,70, 5739-5745

37. Rafiński, Z.; Kozakiewicz, A.; Rafińska, K., (-)-β-pinene-derived N-heterocyclic carbenes : application to highly enantioselective intramolecular Stetter reaction, ACS Catalysis, 2014, 4, 1404-1408.; Highlighted in SynFacts, 2014, 10, 639

36. Krzemiński, M. P. „3-Amino-2,6,6-trimethylbicyclo[3.1.1]heptan-2-ol, (First update)” w eEROS–Encyclopedia of Reagents for Organic Synthesis (DOI: 10.1002/047084289X.rn00063.pub2), Eds. D. Crich, A. B. Charette, P. L. Fuchs, T. Rovis, J. Wiley: New York, opublikowano online 20.10.2014

35. Zaidlewicz, M.; Krzemiński, M. „Norephedrine–Borane (First update)” w eEROS–Encyclopedia of Reagents for Organic Synthesis (DOI: 10.1002/047084289X.rn062.pub2), Eds. D. Crich, A. B. Charette, P. L. Fuchs, T. Rovis, J. Wiley: New York, opublikowano online 27.05.2014

34. Zaidlewicz, M.; Krzemiński, M. „2-Amino-3-methyl-1,1-diphenyl-1-butanol (First update)” w eEROS–Encyclopedia of Reagents for Organic Synthesis (DOI: 10.1002/047084289X.ra092m.pub2), Eds. D. Crich, A. B. Charette, P. L. Fuchs, T. Rovis, J. Wiley: New York, opublikowano online 27.05.2014

33. Piasta, A. M.; Jastrzębska, A.; Krzemiński, M. P.; Muzioł, T. M.; Szłyk, E., New procedure of selected biogenic amines determination in wine samples by HPLC, Analytica Chimica Acta 2014, 834, 58-66

32. Błocka, E.; Bosiak, M. J.; Wełniak, M.; Ludwiczak, A.; Wojtczak, A., Enantioselective cyanosilylation of aldehydes catalyzed by novel camphor derived Schiff bases-titanium(IV) complexes, Tetrahedron: Asymmetry, 2014, 25, 554–562

31. Budny, M.; Nowak, M.; Wojtczak, A.; Wolan, A., Synthesis of N-(2,3,4,5,6-pentafluorobenzyloxy)-γ-lactams by rhodium-catalyzed cyclization of diazo amides Eur. J. Org. Chem., 2014, 29, 6361–6365

30. Ścianowski, J.; Rafalski, J.; Banach A.; Czaplewska, J.; Komoszyńska A., Synthesis and reactions of the optically active selenols derived from monoterpenes, Tetrahedron: Asymmetry, 2013, 24, 1089-1096

29. Ziegler-Borowska, M.; Bosiak, M. J.; Zaidlewicz, M., Kwas 2-amino-6-dihydroksyborylo-1,2,3,4-tetrahydronaftaleno-2-karboksylowy i sposób jego wytwarzania: Patent PL 215215 B1, 2013

28. Bosiak, M. J.; Rakowiecki, M.; Orłowska, K. J.; Kędziera, D. Adams, J., Synthesis and photoluminescent properties of conjugated aryl-vinyl dioctyl 2,6-dimethylbenzofuro[5,6-b]furan-3,7-dicarboxylate derivatives, Dyes and Pigments, 2013, 99, 803-811

27. Kołodziejska, R.; Karczmarska-Wodzka, A.; Wolan, A.; Draminski, M., Candida antarctica lipase B catalyzed enantioselective acylation of pyrimidine acyclonucleoside: Biocatalysis and Biotransformations,2012, 30, 426–430

26. Białek, D.; Kowalski, K.; Ścianowski, J., Rafiński, Z.; Wojtczak, A., Preparation and characterization of new chiral ferrocenyl selenides, J. Organomet. Chem., 2012, 712, 1-6

25. Drabowicz, J.; Lewkowski, J.; Ścianowski, J., Selenium compounds with valency higher than two; Organoselenium chemistry : synthesis and reactions / ed.: Wirth, T./; Weinheim : Wiley-VCH Verlag, 2012, 191-256

24. Krzemiński, M. P.; Ćwiklińska, M.; Kmieciak, A. „Monoterpene-derived 1,2-amino alcohols as catalysts precursors for asymmetric reactions” w „From molecules to functional architecture supramolecular interactions : collected research papers” / Ed. V. I. Rybachenko, East Publisher House, Donetsk 2012, 141-173

23. Jaworska, M.; Pawlak, T.; Kruszyński, R.; Ćwiklińska, M.; Krzemiński, M. P., NMR crystallography comparative studies of chiral (1R,2S,3R,5R)-3-amino-6,6-dimethylbicyclo[3.1.1]heptan-2-ol and its p-toluenesulfonamide derivative, Crystal Growh and Design 2012, 12, 5956-5965

22. Ramachandran, P. V.; Tafelska-Kaczmarek, A.; Chatterjee, A. J. Org. Lett. 2012, 77, 9329-9333

21. Kadac, K.; Bosiak, M. J.; Nowaczyk J., Synthesis and AC impedance studies of 2,6-distyrylbenzofuro[5,6-b]furan based new organic semiconductor, Synthetic Metals, 2012, 162, 1981–1986

20. Bosiak, M. J.; Jakubowska, J. A.; Aleksandrzak, K. B.; Kamiński, S.; Kaczmarek-Kędziera, A.; Ziegler-Borowska, M.; Kędziera, D.; Adams, J., Synthesis of a new class of highly fluorescent aryl-vinyl benzo[1,2-b:4,5-b’]difuran derivatives, Tetrahedron Lett., 2012, 53, 3923-3926

19. Pakulski, M. M.; Mahato S. K.; Bosiak, M. J.; Krzeminski, M. P.; Zaidlewicz M.,Enantioselective reduction of ketoxime ethers with borane-oxazaborolidines and synthesis of the key intermediate leading to (S)-rivastigmine, Tetrahedron: Asymmetry, 2012, 23, 716-721

18. Ziegler-Borowska, M.; Bosiak, M. J.; Kosmalski, T.; Kaczanowska, K.; Zaidlewicz, M., Kwas 2-amino-6-dihydroksyborylo-1,2,3,4-tetrahydronaftaleno-2-karboksylowy i sposób jego wytwarzania, Patent PL393268-A1; PL215215-B1., 2012

17. Bosiak, M. J.; Aleksandrzak, K. B.; Jakubowska, J. A.; Łukaitis, R. Patent PL392858-A1, 2012

16. Krzemiński, M. P.; Ćwiklińska, M., Chiral terpene auxiliaries II. spiroborate esters derived from α-pinene-new catalysts for asymmetric borane reduction of prochiral ketones, Tetrahedron Letters 2011, 51, 332-336

15. Ramachandran, P. V.; Tafelska-Kaczmarek, A.; Sakavuyi, K.; Chatterjee, A., Fluoroallylboration-olefination for the synthesis of (Z)-4,4-difluoropent-2-enoates and 5,5-difluoro-5,6-dihydropyran-2-ones, Org. Lett. 2011, 13, 1302-1305

14. Ramachandran, P. V.; Tafelska-Kaczmarek, A.; Sakavuyi, K., Asymmetric fluoroallylboration of aldehydes, Org. Lett. 2011, 13, 4044-4047

13. Wolan, A.; Soueidan, M.; Chiaroni, A.; Retailleau, P.; Py, S.; Six, Y., Tactics for the asymmetric preparation of 2-azabicyclo[3.1.0]hexane and 2-azabicyclo[4.1.0]heptane scaffolds, Tetrahedron Letters, 2011,52, 2501–2504

12. Wolan, A.; Joachimczak, A.; Budny, M.; Kozakiewicz, A., Zinc-mediated allylation of aldoxime esters, Tetrahedron Lett., 2011, 52, 1195–1198

11. Bosiak, M. J.; Pakulski, M. M., Asymmetric reduction of α-keto aldoxime O-ethers, Synthesis, 2011, 2, 316-324

10. Jędrzejewska, B.; Pietrzak, M.; Rafiński, Z., Phenyltrialkylborates as co-initiators with cyanine dyes in visible light polymerization of acrylates, Polymer, 2011, 52, 2110-2119

9. Krzemiński, M. P, „Sposób redukcji ketonów alkilowoarylowych”, Patent PL 206514 B1, 2010

8. Krzemiński, M. P. „Sposób wytwarzania nowego (1R,2S,3R,5R)-(–)-3-amino-6,6-dimetylo-2-hydroksybicyklo[3.1.1]heptanu”, Patent PL 206513 B1, 2010

7. Veeraraghavan Ramachandran, P.; Biswas, D.; Krzemiński, M. P.; Chen, G.-M., Efficient synthesis of chiral C2-symmetric diamines via allylboration of bis-N,N’-metallodiimines, Tetrahedron Letters 2010, 51, 332-336

6. Collas A., Bagrowska I., Aleksandrzak K., Zeller M., Blockhuys F., Competition between Methoxy-Based and Pyrazine-Based Synthons in Methoxy-Substituted Distyrylpyrazines, Crystal Growth and Design,2011, 11, 1299

5. Mlostoń, G.; Obijalska, E.; Tafelska-Kaczmarek, A.; Zaidlewicz, M., Reactions of α-imino ketones derived from arylglyoxals with (trifluoromethyl)trimethylsilane : a new route to β-amino-α-trifluoromethyl alcohols, J. Fluorine Chem. 2010, 131, 1289-1296

4. Tafelska-Kaczmarek, A.; Prewysz-Kwinto, A.; Skowerski, K.; Pietrasiak, K.; Kozakiewicz, A.; Zaidlewicz, M., Asymmetric synthesis of β-amino alcohols by the transfer hydrogenation of α-keto imines, Tetrahedron: Asymmetry 2010, 21, 2244-2248

3. Wolan, A.; Six, Y., Synthetic transformations mediated by the combination of titanium(IV) alkoxides and Grignard reagents: selectivity issues and recent application, Tetrahedron, 2010, 66, 3097–3133

2. Wolan, A.; Six, Y., Synthetic transformations mediated by the combination of titanium(IV) alkoxides and grignard reagents : selectivity issues and recent applications, Tetrahedron, 2010, 66, 15–61

1. Wang,M.; Holmes-Davis, R.; Blinder, R.; Rafiński, Z.; Jędrzejewska, B.; Pączkowski, J.; Warner,B.; Koshinsky, H., Assays based on detection of photobleaching reaction products from dye catalytic complex, US Appl. Patent, 2010, 20100209909